5.Table 22 – Type D Table 11 Cationic Rapid Setting Emulsified Polymerized Asphalt (CRS-2P) Tests Test Method Min. Max. Emulsion Viscosity , SF, 140º F (60º C), s AASHTO T 59 100 400 (Project-site Acceptance/Rejection Limits) Settlement (a) 5 days, percent AASHTO T 59 5 Storage Stability Test (b) 1 d, 24 h, percent AASHTO T 59 Demulsibility (c) 35 ml, 0.8% sodium dioctyl AASHTO T 59 40 Sulfosucinate, percent Particle Charge Test AASHTO T 59 Positive Sieve Test, percent AASHTO T 59 0.10 Distillation Oil distillate, by volume of emulsion, percent 0 Residue (d), percent 68 Residue from Distillation Test Penetration, 77º F (25º C), 100 g, 5 s, dmm AASHTO T 49 80 150 Ductility, 39.2º F (4º C), 5 cm/min, cm AASHTO T 51 35 Toughness, lb-in ASTM D 5801 75 Tenacity, lb-in ASTM D 5801 50 Solubility in trichloroethylene, percent AASHTO T 44 97.5 (a) The test requirement for settlement may be waived when the emulsified asphalt is used in less than a five-day time unless the purchaser requires the test. (b) The 24-hour (1-day) storage stability test may be used instead of the five day settlement test. (c) The demulsibility test is made within 30 days from date of shipment. (d) Distillation is determined by AASHTO T 59 with modifications to include a 350 ± 5º F (177 ± 3º C) maximum temperature to be held for 15 minutes. Modify the asphalt cement before emulsification. Table 12 Latex Modified Cationic Rapid Setting Emulsified Asphalt (LMCRS-2) Tests Test Method Min. Max. Emulsion Viscosity, SF, 122º F (50º C), s AASHTO T 59 140 400 (Project Site Acceptance/Rejection Limits) Settlement (a) 5 days, percent AASHTO T 59 5 Storage Stability Test (b) 1 d, 24 h, percent AASHTO T 59 1 Demulsibility (c) 35 ml, 0.8% sodium Dioctyl AASHTO T 59 40 Sulfosucinate, percent Particle Charge Test AASHTO T 59 Positive Sieve Test, percent AASHTO T 59 0.3 Distillation Oil distillate, by volume of emulsion, percent 0 Residue (d), percent 65 Residue from Distillation Test Penetration, 77º F (25º C), 100 g, 5 s, dmm AASHTO T 49 40 200 Torsional Recovery (e) 18 (a) The test requirement for settlement may be waived when the emulsified asphalt is used in less than a five-day time unless the purchaser requires the test. (b) May use the 24-hour (1-day) storage stability test instead of the five-day settlement test. (c) Make the demulsibility test within 30 days from date of shipment. (d) Determine distillation by AASHTO T 59, with modifications to include a 350 ± 5ºF (177±3ºC) maximum temperature to be held for 15 minutes. (e) CA 332 (California Test Method) Co-mill latex and asphalt during emulsification Table 13 Cationic Medium Setting Emulsified Asphalt (CMS-2S) Tests Test Method Specification Emulsion Viscosity, SF, 122º F (50º C), s AASHTO T 59 50 - 450 Percent residue AASHTO T 59 60 min Storage Stability Test, 1d, 24h, percent AASHTO T 59 1 max Sieve, percent AASHTO T 59 0.10 max Particle charge AASHTO T 59 Positive Oil Distillate, percent by volume of emulsion AASHTO T 59 5-15 Residue Penetration, 77º F (25º C), 100g, 5 sec, dmm AASHTO T 59 100-250 Solubility, percent AASHTO T 59 97.5 min. Table 14 High Float Medium Setting Emulsified Asphalt ( HFMS-2) Tests Test Method Min. Max. Emulsion Viscosity, SF, 122° F (50° C), s AASHTO T 59 70 300 (Project Site Acceptance/Rejection Limits Storage Stability Test, 1d, 24 h, percent AASHTO T 59 1.0 Sieve Test , percent AASHTO T 59 0.1 Distillation Oil Distillate, by volume of emulsion, percent AASHTO T 59 NA NA Residue, percent AASHTO T 59 65 Residue from Distillation Test Penetration, 77° F (25° C), 100g, 5 s, dmm AASHTO T 49 50 200 Float Test, 140° F (60° C), s AASHTO T 50 1,200 Solubility in Trichloroethylene, percent AASHTO T 44 97.5 Ductility, 77° F (25° C) 5cm/min, cm AASHTO T 51 40 Table 15 High Float Medium Setting Emulsified Polymerized Asphalt (HFMS-2P) (a) Tests Test method Min. Max. Emulsion Viscosity, SF, 122º F (50º C), s AASHTO T 59 100 450 (Project Site Acceptance/Rejection Limits) Storage Stability Test, 1 d, 24 h, percent AASHTO T 59 1.0 Sieve Test, percent AASHTO T 59 0.1 Distillation Oil distillate, by volume of emulsion, percent AASHTO T 59 7 Residue (b), percent AASHTO T 59 65 Residue from Distillation Test Penetration, 77º F (25º C), 100 g, 5 s, dmm AASHTO T 49 70 300 Float Test, 140º F (60º C), s AASHTO T 50 1,200 Solubility in trichloroethylene, percent AASHTO T 44 97.5 Elastic Recovery, 77º F (25º C), percent AASHTO T 301 50 (a) Supply an HFMS-2P (anionic, polymerized, high-float) as an emulsified blend of polymerized asphalt cement, water, and emulsifiers. Polymerize the asphalt cement with at least 3.0% polymer by weight of the asphalt cement before emulsification. The emulsion must be smooth and homogeneous throughout with no white, milky separation, pumpable, and suitable for application through a distributor after standing undisturbed for at least 24 hours. (b) Determine the distillation by AASHTO T 59, with modifications to include a 350 ± 5º F (177 ± 3º C) maximum temperature to be held for 15 minutes. Table 16 High Float Medium Setting Emulsified Polymerized Asphalt (HFMS-2SP) (a) Tests Test method Min. Max. Emulsion Viscosity, SF, 122º F (50º C), s AASHTO T 59 50 450 (Project Site Acceptance/Rejection Limits) Storage Stability Test, 1 d, 24 h, percent AASHTO T 59 1 Sieve Test, percent AASHTO T 59 0.1 Distillation Oil distillate, by volume of emulsion, percent AASHTO T 59 7 Residue (b), percent AASHTO T 59 65 Residue from Distillation Test Penetration, 77º F (25º C), 100 g, 5 s, dmm AASHTO T 49 150 300 Float Test, 140ºF (60ºC), s AASHTO T 50 1200 Solubility in trichloroethylene, percent AASHTO T 44 97.5 Elongation Recovery(c), 77º F (25º C), percent AASHTO T 301 50 (a) Supply an HFMS-2SP (anionic, polymerized, high-float) as an emulsified blend of polymerized asphalt cement, water, and emulsifiers. Polymerize the asphalt cement with at least 3.0% polymer by weight of the asphalt cement before emulsification. The emulsion must be smooth and homogeneous throughout with no white, milky separation, pumpable, and suitable for application through a distributor after standing undisturbed for at least 24 hours. (b) Determine the distillation by AASHTO T 59, with modifications to include a 350 ± 5º F (177 ± 3º C) maximum temperature to be held for 15 minutes. (c) Report only when penetration is greater than 300 dmm. Table 17 High Float Rapid Setting Emulsified Polymerized Asphalt (HFRS-2P) (a) Tests Test method Min. Max. Emulsion Viscosity, SF @ 122º F (50º C), s AASHTO T 59 50 450 (Project Site Acceptance/Rejection Limits) Storage Stability Test (b) 1 d, 24 h, percent AASHTO T 59 1 Demulsibility 0.02 N Ca Cl2, percent AASHTO T 59 40 Sieve Test, percent AASHTO T 59 0.1 Distillation Oil distillate, by volume of emulsion, percent AASHTO T 59 3 Residue (b), percent AASHTO T 59 65 Residue from Distillation Test Penetration, 77º F (25º C), 100 g, 5 s, dmm AASHTO T 49 70 150 Float Test, 140º F (60º C), s AASHTO T 50 1,200 Solubility in trichloroethylene, percent AASHTO T 44 97.5 Elastic Recovery, 77º F (25º C), percent AASHTO T 301 58 (a) Supply an HFMS-2SP (anionic, polymerized, high-float) as an emulsified blend of polymerized asphalt cement, water, and emulsifiers. Polymerize the asphalt cement with at least 3.0% polymer by weight of the asphalt cement before emulsification. The emulsion must be smooth and homogeneous throughout with no white, milky separation, pumpable, and suitable for application through a distributor after standing undisturbed for at least 24 hours. (b) Determine the distillation by AASHTO T 59, with modifications to include a 350 ± 5ºF (177±3ºC) maximum temperature to be held for 15 minutes. Table 18 Cationic Rapid Setting Emulsified Asphalt (CRS-2A,B) Tests Test Method Min Max Emulsion Viscosity, SF, 122º F (50º C), s AASHTO T 59 140 400 (Project Site Rejection/Acceptance Limits) Storage stability test, 24 h, percent AASHTO T 59 1 Demulsibility, 35 mL 0.8 percent Sodium AASHTO T 59 Dioctyl Sulfosucinate, percent 40 Particle charge test AASHTO T 59 Positive Sieve test, percent AASHTO T 59 0.10 Distillation Oil distillate, by volume of emulsion, percent AASHTO T 59 0 Residue, percent AASHTO T 59 65 Use PG58-22 and PG64-22 as base asphalt cement for CRS-2A, B, respectively. Specification for high temperature performance – original and RTFO G*/sinδ within 3º C of grade. Table 19 Emulsified Asphalt Pavement Rejuvenating Agent Concentrate Type A Property Test Method Limits Viscosity, SF, 77º F (25º C), s AASHTO T 59 15 Min 40 Max Residue , percent W (a) AASHTO T 59 60 Min. 65 Max. Miscibility Test (b) AASHTO T 59 No Coagulation Sieve Test, percent W ( c) AASHTO T 59 0.20 Max. 5-day Settlement, percent W AASHTO T 59 5.0 Max. Particle Charge AASHTO T 59 Positive Light Transmittance , % UDOT MOI 8-973 30 Max. Cement Mixing AASHTO T 59 2 Max. Residue from Distillation (a) Viscosity, 140º F (60º C), mm2/s ASTM D 4402 150 - 300 Flash Point, COC, º F (º C) AASHTO T 48 385 Min. Asphaltenes, percent W ASTM D 2006 0.4 Min. 0.75 Max. Maltene Distribution Ratio ASTM D 2006 0.3 Min. 0.6 Max (PC + A1)/(S + A2) (d) Saturated Hydrocarbons, S (d) ASTM D 2006 21 Min. 28 Max. PC/S Ratio (d) ASTM D 2006 1.5 Min. (a) AASHTO T 59, Evaporation Test, modified as follows: Heat a 50 gram sample to 300ºF until foaming ceases, then cool immediately and calculate results. (b) AASHTO T 59, modified as follows: Use a 0.02 Normal Calcium Chloride solution in place of distilled water. (c) AASHTO T 59, modified as follows: Use distilled water in place of a two percent sodium oleate solution. (d) Chemical composition by ASTM Method D-2006-70: PC= Polar Compounds, A1 = First Acidaffins A2 = Second Acidaffins, S = Saturated Hydrocarbons Table 20 Emulsified Asphalt Pavement Rejuvenating Agent Concentrate Type B Tests Test Method Limits Viscosity, SF, 77º F (25º C), s AASHTO T 59 25 - 150 Residue, percent W AASHTO T 59 (mod) (a) 62 Min. Sieve Test, percent W AASHTO T 59 0.10 Max. 5-day Settlement AASHTO T 59 5.0 Max. Particle Charge AASHTO T 59 Positive Pumping Stability (b) Pass Residue from Distillation (a) Viscosity @ 140º F (60º C), mm2/s AASHTO T 201 2,500 - 7,500 Solubility in 1,1,1 Trichloroethylene, AASHTO T 44 98 Min. percent Flash Point, COC AASHTO T 48 204º C, Min. Asphaltenes, percent W ASTM D 2007 15 Max. Saturates, percent W ASTM D 2007 30 Max. Aromatics, percent W ASTM D 2007 25 Min. Polar Compounds, percent W ASTM D 2007 25 Min. (a) Determine the distillation by AASHTO T 59 with modifications to include a 300 ± 5º F (149 ± 3º C) maximum temperature to be held for 15 minutes. (b) Test pumping stability by pumping 475 ml of Type B diluted 1 part concentrate to 1 part water, at 77º F (25º C) through a ¼ inch gear pump operating at 1750 rpm for 10 minutes with no significant separation or coagulation in pumped material. Type B – an emulsified blend of lube oil or lube oil extract and petroleum asphalt. Table 21 Emulsified Asphalt Pavement Rejuvenating Agent Concentrate Type B Modified Property Test Method Limits Viscosity, SF, 77º F (25º C), s AASHTO T 59 50 - 200 Residue(a), percent W AASHTO T 59 62 Min. Sieve Test, percent W AASHTO T 59 0.20 Max. 5-day Settlement, percent W AASHTO T 59 5.0 Max. Particle Charge AASHTO T 59 Positive Pumping Stability (b) Pass Residue from Distillation (a) Viscosity (c) 275º F (135º C), cP ASTM D 4402 150 - 300 Penetration, 77º F (25º C), dmm AASHTO T 49 180 Min. Solubility in 1,1,1 Trichloroethylene, AASHTO T 44 98 Min. percent Flash Point, COC, º F (º C) AASHTO T 48 400(204) Min. Asphaltenes, percent W ASTM D 2007 20 - 40 Saturates, percent % W ASTM D 2007 20 Max. Polar Compounds, percent W ASTM D 2007 25 Min. Aromatics, percent W ASTM D 2007 20 Min. PC/S Ratio ASTM D 2007 1.5 Min. (a) Determine the distillation by AASHTO T 59 with modifications to include a 300±5ºF (149 ± 3º C) maximum temperature to be held for 15 minutes. (b) Pumping stability is tested by pumping 475 ml of Type B diluted 1 part concentrate to 1 part water, at 77º F (25º C) through a ¼ inch gear pump operating at 1750 rpm for 10 minutes with no significant separation or coagulation in pumped material. (c) Brookfield Thermocel Apparatus-LV model. ≥ 50 rpm with a #21 spindle, 7.1 g residue, at > 10 torque As required by the Asphalt Emulsion Quality Management Plan 508, UDOT Minimum Sampling and Testing Requirements, the supplier certifies that the base stock contains at least 15% by weight of Gilsonite Ore. Use the HCL precipitation method as a qualitative test to detect the presence of Gilsonite. Table 22 Emulsified Asphalt Pavement Rejuvenating Agent Concentrate Type C Property Test Method Limits Viscosity, SF, 77º F (25º C), s AASHTO T 59 10 - 100 Residue (a), percent W (Type C supplied 30 Min. 1:1 AASHTO T 59 ready to use 1:1 or 2:1. 40 Min. 2:1 Sieve Test, percent W (b) 0.10 Max. 5-day Settlement, percent W AASHTO T 59 5.0 Max. Particle Charge AASHTO T 59 Positive pH (May be used if particle charge test is inconclusive) 2.0 - 7.0 Pumping Stability (c) Pass Tests of Residue from Distillation (a) Viscosity, 275º F (135º C), mm2/s AASHTO T 201 475 - 1,500 Solubility in 1,1,1 Trichloroethylene, AASHTO T 44 97.5 Min. percent RTFO mass loss, percent W AASHTO T 240 2.5 Max. Specific Gravity AASHTO T 228 0.98 Min. Flash Point, COC AASHTO T 48 232º C, Min. Asphaltenes, percent W ASTM D 2007 25 Min., 45 Max. Saturates, percent W ASTM D 2007 10 Max. Polar Compounds, percent W ASTM D 2007 30 Min. Aromatics, percent W ASTM D 2007 15 Min. (a) Determine the distillation by AASHTO T 59 with modifications to include a 300 ± 5º F (149 ± 3º C) maximum temperature to be held for 15 minutes. (b) Test method identical to AASHTO T 59 except that distilled water is used in place of 2% sodium oleate solution. (c) Test pumping stability by pumping 475 ml of Type diluted 1 part concentrate to 1 part water, at 77º F (25º C) through a ¼ inch gear pump operating at 1750 rpm for 10 minutes with no significant separation or coagulation in pumped material. As required by the Asphalt Emulsion Quality Management Plan Section 508 , UDOT Minimum Sampling and Testing Requirements,, the supplier certifies that the base stock contains at least 10% by weight of Gilsonite ore. Use the HCL precipitation method as a qualitative test to detect the presence of Gilsonite. Table 23 Emulsified Asphalt Pavement Rejuvenating Agent Concentrate Type D Property Test Method Limits Viscosity, SF, 77º F (25º C), s AASHTO T 59 30 - 90 Residue, (b) percent W AASHTO T 59 65 Sieve Test, percent W AASHTO T 59 0.10 Max. pH 2.0 - 5.0 Residue from Distillation (b) Viscosity, 140º F (60º C), cm2/s AASHTO T 201 300 - 1200 Viscosity, 275º F (135º C), mm2/s AASHTO T 201 300 Min. Modified Torsional Recovery (a) percent CA 332 (Mod) 40 Min. Toughness, 77º F (25º C), in-lb ASTM D 5801 8 Min. Tenacity, 77º F (25º C), in-lb ASTM D 5801 5.3 Min. Asphaltenes, percent W ASTM D 2007 16 Max. Saturates, percent W ASTM D 2007 20 Max. (a) Torsional recovery measurement to include first 30 seconds. (b) Determine the distillation by AASHTO T 59 with modifications to include a 300 ± 5º F (149 ± 3º C) maximum temperature to be held for 15 minutes.